Protocol for fabrication and characterization of Fe-SAC@COF for electrocatalytic oxygen evolution reaction

STAR Protoc. 2022 Aug 18;3(3):101626. doi: 10.1016/j.xpro.2022.101626. eCollection 2022 Sep 16.


Single-atom catalysts (SACs) have promising atomic utilization efficiency and catalytic activity, but their construction with a specific coordination mode remains challenging. This protocol describes the synthesis of a coordinated Fe-SAC@COF for boosted electrocatalytic oxygen evolution reaction (OER). We also detail the steps for single iron atoms confinement and characterization of the COF and Fe-SAC@COF with X-ray diffraction and transmission electron microscopy technique. For complete details on the use and execution of this protocol, please refer to Wang et al. (2022).

PMID:36035801 | PMC:PMC9405112 | DOI:10.1016/j.xpro.2022.101626


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